in anhydrous butyl ether
dropping PI(CF3)2 to AlH3 in di-butylether and heating mixture to 70°C;;
参考文献
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3896 - 3904
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Burg, A. B.; et al.
WADC-TR-56-82 (1957), Tl. 1, (1958), Tl. 2, S. 31
Griffiths,J.E.; Burg,A.B.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3442 - 3450
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Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3896 - 3904
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Gmelin Handbook: F: PerFHalOrg.3, 1.2, page 14 - 30
in neat (no solvent)
shaking starting material;; removal of PCl(CF3)2 with H2O;;
参考文献
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3896 - 3904
Full Text View citing articles Show Details
Burg, A. B.; et al.
WADC-TR-56-82 (1957), Tl. 1, (1958), Tl. 2, S. 31
hydrogenchloride
in Carius tube, in darkness, 20°C, 26 d;
参考文献
Dobbie, R. C.; Hopkins, M. J.
Journal of Fluorine Chemistry, 1973 , vol. 3, p. 367 - 374
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Gmelin Handbook: F: PerFHalOrg.3, 1.13, page 160 - 160
