1-Boc-4-甲酰基吲哚合成路线 (共 4 条)
反应条件
potassium tert-butylate
T=0 - 20°C; 72 h;
参考文献
Carlier, Paul R.; Lam, Polo C.-H.; Wong, Dawn M.
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6256 - 6259
反应条件
diisobutylaluminium hydride in dichloromethane
T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Zhang, Min; Tang, Weiping
Organic Letters, 2012 , vol. 14, # 14 p. 3756 - 3759
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Min; Tang, Weiping
Organic Letters, 2012 , vol. 14, # 14 p. 3756 - 3759
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Min; Tang, Weiping
Organic Letters, 2012 , vol. 14, # 14 p. 3756 - 3759