N,N′-双(3-氨丙基)-1,3-丙二胺合成路线 (共 10 条)
反应条件
ammonia; hydrogen; W-2 Raney Ni in methanol Catalytic hydrogenation; P=2700 Torr; 65 h;
参考文献
Garrett, Shane W.; Davies, Owen R.; Milroy, David A.; Wood, Pauline J.; Pouton, Colin W.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 7 p. 1779 - 1797
反应条件
palladium T=120°C; 12 h;
参考文献
Murahashi; Yoshimura; Tsumiyama; Kojima
Journal of the American Chemical Society, 1983 , vol. 105, # 15 p. 5002 - 5011
反应条件
borane-THF in tetrahydrofuran 7 h; Heating;
参考文献
Rubio, Mercedes; Astorga, Covadonga; Alfonso, Ignacio; Rebolledo, Francisca; Gotor, Vicente
Synthetic Communications, 2002 , vol. 32, # 16 p. 2441 - 2452
反应条件
1: NH3 / methanol / 7 °C 2: BH3*THF / tetrahydrofuran / 7 h / Heating View Scheme
参考文献
Rubio, Mercedes; Astorga, Covadonga; Alfonso, Ignacio; Rebolledo, Francisca; Gotor, Vicente
Synthetic Communications, 2002 , vol. 32, # 16 p. 2441 - 2452
反应条件
hydrogen T=100 - 200°C; P=0 - 15001.5 Torr; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2006/82203 A1, 2006 ;
Location in patent: Page/Page column 2; 3; 9 ;
反应条件
Thermus thermophilus triamine/agmatine aminopropyltransferase; DL-threo-1,4-dimercapto-2,3-butanediol T=37°C; pH=9; aq. bufferEnzymatic reaction; Kinetics;
参考文献
Ohnuma, Mio; Ganbe, Tadashi; Terui, Yusuke; Niitsu, Masaru; Sato, Takao; Tanaka, Nobuo; Tamakoshi, Masatada; Samejima, Keijiro; Kumasaka, Takashi; Oshima, Tairo
Journal of Molecular Biology, 2011 , vol. 408, # 5 p. 971 - 986
反应条件
ammonium hydroxide T=50°C; E(a); Rate constantThermodynamic data;
参考文献
Chernitskii, K. V.; Bobylev, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 8.2 p. 1862 - 1867,1720 - 1724
参考文献
Whitby et al.
Industrial and Engineering Chemistry, 1950 , vol. 42, p. 445,455
反应条件
ammonium hydroxide T=50°C; E(a); Rate constantThermodynamic data;
参考文献
Chernitskii, K. V.; Bobylev, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 8.2 p. 1862 - 1867,1720 - 1724
反应条件
formic acid Mechanism;
参考文献
Tetrahedron Letters, , vol. 32, # 52 p. 7755 - 7758