N,N'-二-2-吡啶甲基乙二胺合成路线 (共 7 条)
反应条件
sodium cyanoborohydride; trifluoroacetic acid in methanol; diethyl ether T=25°C; 11 h;
参考文献
Kumar, Pankaj; Kalita, Apurba; Mondal, Biplab
Dalton Transactions, 2013 , vol. 42, # 16 p. 5731 - 5739
反应条件
1: calcium chloride / diethyl ether 2: sodium cyanoborohydride; trifluoroacetic acid; calcium chloride / methanol View Scheme
参考文献
Vad, Mads S.; Nielsen, Anne; Lennartson, Anders; Bond, Andrew D.; McGrady, John E.; McKenzie, Christine J.
Dalton Transactions, 2011 , vol. 40, # 40 p. 10698 - 10707
反应条件
sodium hydroxide; trimethylhexadecylammonium chloride in water 24 h; Ambient temperature;
参考文献
Synthesis, , # 6 p. 539 - 540
反应条件
formic acid Heating;
参考文献
Che, Chi-Ming; Tang, Wai-Tong; Wong, Kwok-Yin; Wong, Wing-Tak; Lai, Ting-Fong
Journal of Chemical Research, Miniprint, 1991 , # 2 p. 401 - 427
反应条件
hydrogen; palladium on activated charcoal in methanol
P=2585.74 Torr; 24 h;
参考文献
Vachet, Richard W.; Hartman, Judith Ann R.; Callahan, John H.
Journal of Mass Spectrometry, 1998 , vol. 33, # 12 p. 1209 - 1225
反应条件
sodium tetrahydroborate in methanol
参考文献
Hosseinzadeh, Rahman; Golchoubian, Hamid; Masoudi, Mahtab
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 3 p. 649 - 653
反应条件
1: ethanol / 10 h / Heating
2: NaBH4, borax / methanol
View Scheme
参考文献
Che, Chi-Ming; Tang, Wai-Tong; Wong, Kwok-Yin; Wong, Wing-Tak; Lai, Ting-Fong
Journal of Chemical Research, Miniprint, 1991 , # 2 p. 401 - 427