1: 17.1 g / palladium(II) acetate, triphenylphosphine, tributylamine / xylene / 5 h / 105 °C 2: 75 percent / NiCl2*6H2O, sodium borohydride / methanol / 1.67 h / 20 °C 3: 96 percent / polyphosphoric acid / 1.17 h / 80 °C View Scheme
参考文献
Novak, J.; Salemink, C. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2403 - 2406
1: With isopropylmagnesium chloride; lithium chloride in tetrahydrofuran T=-15°C; 0.25 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=0°C; 2 h; 3: With ammonia; iodine in tetrahydrofuran; water T=20°C; 2 h;