N-苄基-N-(仲-丁基)胺盐酸盐合成路线 （共 11 条）
反应条件
1: aq.-ethanolic ammonia View Scheme
参考文献
Labriola; Dorronsoro; Verruno
Anales de la Asociacion Quimica Argentina (1921-2001), 1949 , vol. 37, p. 79,84
参考文献
Labriola; Dorronsoro; Verruno
Anales de la Asociacion Quimica Argentina (1921-2001), 1949 , vol. 37, p. 79,84
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 1,3-bis-(diphenylphosphino)propane; potassium carbonate in toluene
T=110°C; 12 h; Molecular sieveInert atmosphereSchlenk technique; chemoselective reaction;
参考文献
Tamaddoni Jahromi, Bahareh; Kharat, Ali Nemati
Journal of Coordination Chemistry, 2013 , vol. 66, # 19 p. 3498 - 3508
反应条件
iridium bromide; sulfuric acid; zinc in 1,4-dioxane; water
T=30°C; 72 h;
参考文献
da Silva, Renato A.; Bieber, Lothar W.
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 689 - 691
反应条件
hydrogen; magnesium oxide; copper
T=220°C; P=11250.9 Torr;
参考文献
Tarasevich; Kozlov
Russian Journal of General Chemistry, 2004 , vol. 74, # 3 p. 379 - 383
反应条件
methyllithium in diethyl ether; hexane; cyclohexane
1.) -78 deg C, 20 min, 2.) from -78 to -15 deg C, 2 h;
参考文献
Beak, Peter; Selling, Gordon W.
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5574 - 5580
反应条件
sodium tetrahydroborate in methanol
2 h;
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
1: P2S5 / dioxane / 2 h / Ambient temperature
2: tetrahydrofuran / Ambient temperature
3: 44 percent Chromat. / NaBH4 / methanol / 2 h
View Scheme
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
1: tetrahydrofuran / Ambient temperature
2: 44 percent Chromat. / NaBH4 / methanol / 2 h
View Scheme
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; sodium hydroxide
T=120°C; 48 h; Inert atmosphere;
参考文献
Werkmeister, Svenja; Bornschein, Christoph; Junge, Kathrin; Beller, Matthias
European Journal of Organic Chemistry, 2013 , # 18 p. 3671 - 3674
