(NH4)2S; CF3O3S(1-)*Cl3Ti(1+); [N-butylthiazolium][Br] T=80°C; 1 h; Ionic liquid; chemoselective reaction;

acetyl chloride; zinc oxide 0.5 h; Heating;

nickel(II) dichloride dihydrate in acetonitrile T=80°C; Molecular sieveInert atmosphere;

暂无反应条件数据

nickel(II) dichloride dihydrate in acetonitrile T=80°C; Molecular sieveInert atmosphere;

hydroxylamine hydrochloride

hydroxylamine hydrochloride; sodium hydroxide in methanol; water T=20°C; 0.5 h;

potassium tert-butylate in tetrahydrofuran; dimethyl sulfoxide (Ar); addn. of tert-BuONO to Cr-complex at room temp. with stirring; addn. of tert-BuOK (THF); addn. of tert-BuONO after 15 min; stirring for 20 min; hydrolysis with ice; E:Z = 72:28; extn. with ether; washing (H2O); drying (MgSO4); chromy. (silica gel, ether/pentane);