2-[十二烷硫基(硫代羰基)硫基]-2-甲基丙酸合成路线 (共 6 条)
反应条件
1: carbon disulfide; acetone; lauryl mercaptan With sodium hydroxide; Aliquatreg; 336; octadecyl-trimethylammonium chloride in water
0.333333 h;
2: chloroform With sodium hydroxide in water
T=15 - 20°C;
3: With hydrogenchloride in water
参考文献
Liu, Zhilei; Hu, Jiwen; Sun, Jianping; He, Guping; Li, Yinghui; Zhang, Ganwei
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 16 p. 3573 - 3586
反应条件
1: carbon disulfide; acetone; lauryl mercaptan With potassium hydroxide; tetrabutylammomium bromide
0.5 h;
2: chloroform With potassium hydroxide
T=0 - 20°C;
参考文献
Harrisson, Simon; Wooley, Karen L.
Chemical Communications, 2005 , # 26 p. 3259 - 3261
反应条件
1: acetone; lauryl mercaptan With Aliquatreg; 336; sodium hydroxide in water
T=9.84°C; Inert atmosphere;
2: carbon disulfide in water
Inert atmosphere;
3: anhydrous methyl chloride With sodium hydroxide in water
Inert atmosphere;
参考文献
Zuluaga, Fabio; Grande, Carlos; Cobo, Justo; Glidewell, Christopher
Acta Crystallographica Section C: Crystal Structure Communications, 2010 , vol. 66, # 12 p. o627-o630
反应条件
1: lauryl mercaptan With potassium phosphate in acetone
0.5 h;
2: carbon disulfide in acetone
0.333333 h;
3: 2-bromo-2-methyl-propionic acid in acetone
21 h;
参考文献
Summers, Matthew J.; Phillips, Daniel J.; Gibson, Matthew I.
Chemical Communications, 2013 , vol. 49, # 39 p. 4223 - 4225
参考文献
Skey, Jared; O'Reilly, Rachel K.
Chemical Communications, 2008 , # 35 p. 4183 - 4185
反应条件
[14C]-Tetramethylammonium bromide in chloroform
Acidic conditions;
参考文献
Johnson, Renjith P.; Jeong, Young-Il; John, Johnson V.; Chung, Chung-Wook; Kang, Dae Hwan; Selvaraj, Manickam; Suh, Hongsuk; Kim, Il
Biomacromolecules, 2013 , vol. 14, # 5 p. 1434 - 1443