1: With caesium carbonate in ethanol 2: With Merryfield resin in N,N-dimethyl-formamide T=50°C; 72 h; 3: With di(n-butyl)tin oxide in chlorobenzene T=133°C; 18 h; Further stages. Further byproducts.;
参考文献
Ruddick, Clare L.; Hodge, Philip; Cook, Anthony; McRiner, Andrew J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 5 p. 629 - 637
1: pyridine / 0 °C
2: NaI / acetone / 2 h / Heating
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
Hang, Howard C.; Geutjes, Ernst-Jan; Grotenbreg, Gijsbert; Pollington, Annette M.; Bijlmakers, Marie Jose; Ploegh, Hidde L.
Journal of the American Chemical Society, 2007 , vol. 129, # 10 p. 2744 - 2745