2-乙氧基-8-甲氧基喹啉合成路线 (共 37 条)
反应条件
1: sodium amalgam; alcohol 2: diluted mineral acid View Scheme
参考文献
Friedlaender; Weinberg
Chemische Berichte, 1882 , vol. 15, p. 1422
参考文献
Illuminati; Gilman
Journal of the American Chemical Society, 1949 , vol. 71, p. 3349
参考文献
Knorr
Chemische Berichte, 1897 , vol. 30, p. 931
反应条件
acetic acid; potassium iodide T=110°C; 4 h;
参考文献
Sridhar Reddy, Maddi; Thirupathi, Nuligonda; Babu, Madala Hari
European Journal of Organic Chemistry, 2012 , # 29 p. 5803 - 5809
反应条件
P=0.1 Torr; Pyrolysis; Title compound not separated from byproducts;
参考文献
Lister, Troy; Prager, Rolf H.; Tsaconas, Michael; Wilkinson, Kerry L.
Australian Journal of Chemistry, 2003 , vol. 56, # 9 p. 913 - 916
反应条件
T=376.8 - 439.8°C; Kinetics;
参考文献
Al-Awadi, Nouria; Taylor, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1589 - 1592
参考文献
Friedlaender; Ostermaier
Chemische Berichte, 1882 , vol. 15, p. 335
参考文献
Illuminati; Gilman
Journal of the American Chemical Society, 1949 , vol. 71, p. 3349
参考文献
Friedlaender; Ostermaier
Chemische Berichte, 1882 , vol. 15, p. 335
反应条件
1: ethyl ethynyl ether With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; 4.33333 h; Inert atmosphere;
2: 2-amino-benzaldehyde in tetrahydrofuran; hexane
T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
Sridhar Reddy, Maddi; Thirupathi, Nuligonda; Babu, Madala Hari
European Journal of Organic Chemistry, 2012 , # 29 p. 5803 - 5809