反应条件
hydrogenchloride; sec.-butyllithium in tetrahydrofuran BuLi add. to org. compd. soln. at -78°C (N2)=, stirring 2 h at same temp., B-compd. addn. over 5 min. mixt. stirring (-78°C/2 h, room temp./overnight, N2), acidifying (HCl), H2O addn., extn. (Et2O), extracts shaking (3 M HCl, brine); drying (Na2SO4), solvent evapn. (water bath, 35°C), air drying overnight at room temp., stirring with ice-cold pentane (washings discarding), air drying overnight;
参考文献
Koen, Mark J.; Morgan, Jacqueline; Pinhey, John T.; Sherry, Christopher J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 4 p. 487 - 491
