3-(苯甲酰氧基)-2,4-戊烷二酮合成路线 （共 6 条）
反应条件
hydrazine hydrate in ethanol 1 h; Ambient temperature;
参考文献
Lloris, Maria E.; Galvez, Nicanor; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron, 1991 , vol. 47, # 37 p. 8031 - 8042
反应条件
1: 20 percent / NaOAc / dimethylformamide / 100 °C 2: 98 percent / KOH / ethanol / 10 h / Heating View Scheme
参考文献
Valgimigli, Luca; Brigati, Giovanni; Pedulli, Gian Franco; DiLabio, Gino A.; Mastragostino, Marina; Arbizzani, Catia; Pratt, Derek A.
Chemistry - A European Journal, 2003 , vol. 9, # 20 p. 4997 - 5010
反应条件
1: benzoic acid With potassium hydroxide in N,N-dimethyl-formamide
T=50°C; 1 h;
2: 3-chloropentane-2,4-dione in N,N-dimethyl-formamide
T=50°C;
参考文献
ARRAY BIOPHARMA INC.
Patent: WO2009/42435 A1, 2009 ;
Location in patent: Page/Page column 113; 116; 119-120 ;
WO 2009/042435 A1
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in ethyl acetate
T=20 - 75°C; 24 h;
参考文献
Uyanik, Muhammet; Suzuki, Daisuke; Yasui, Takeshi; Ishihara, Kazuaki
Angewandte Chemie - International Edition, 2011 , vol. 50, # 23 p. 5331 - 5334
反应条件
in dimethyl sulfoxide
3 h;
参考文献
Valgimigli, Luca; Brigati, Giovanni; Pedulli, Gian Franco; DiLabio, Gino A.; Mastragostino, Marina; Arbizzani, Catia; Pratt, Derek A.
Chemistry - A European Journal, 2003 , vol. 9, # 20 p. 4997 - 5010
反应条件
in chloroform
24 h; Heating;
参考文献
Lloris, Maria E.; Galvez, Nicanor; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron, 1991 , vol. 47, # 37 p. 8031 - 8042
