1-(4-溴-1-萘基)乙酮合成路线 （共 13 条）
参考文献
Baraldi, Pier Giovanni
Patent: US2001/47008 A1, 2001 ;
反应条件
1: 94 percent / NaOCl / H2O / 4.5 h / Heating
2: 25 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h; 2.) room temperature, 14 h
3: 64 percent
View Scheme
参考文献
Dixon, Elisabeth A.; Fischer, Alfred; Robinson, Frank P.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2629 - 2641
反应条件
1: 94 percent / NaOCl / H2O / 4.5 h / Heating
2: 25 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h; 2.) room temperature, 14 h
3: 84.5 percent / PBr3, pyridine / benzene / 6 h / 55 °C
View Scheme
参考文献
Dixon, Elisabeth A.; Fischer, Alfred; Robinson, Frank P.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2629 - 2641
