联苯基[4-(1H,1H,2H,2H-全氟癸基)苯基]膦合成路线 （共 3 条）
反应条件
alane-N,N-dimethylamine in toluene T=90°C; 3 h;
参考文献
Dandapani, Sivaraman; Curran, Dennis P.
Tetrahedron, 2002 , vol. 58, # 20 p. 3855 - 3864
反应条件
1.1: t-BuLi / diethyl ether; pentane / 1 h / -40 °C 1.2: diethyl ether; pentane / -40 - 20 °C 2.1: 0.88 g / alane-N,N-dimethylamine / toluene / 3 h / 90 °C View Scheme
参考文献
Dandapani, Sivaraman; Curran, Dennis P.
Tetrahedron, 2002 , vol. 58, # 20 p. 3855 - 3864
195324-88-01-溴-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟癸基)苯
→
反应条件
1.1: t-BuLi / diethyl ether; pentane / 1 h / -40 °C 1.2: diethyl ether; pentane / -40 - 20 °C 2.1: 0.88 g / alane-N,N-dimethylamine / toluene / 3 h / 90 °C View Scheme
参考文献
Dandapani, Sivaraman; Curran, Dennis P.
Tetrahedron, 2002 , vol. 58, # 20 p. 3855 - 3864
