6-甲基-5-庚烯-2-醇合成路线 (共 96 条)
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h;
参考文献
Mermet-Mouttet, Marie-Paule; Gabriel, Kiroubagaranne; Heissler, Denis
Tetrahedron Letters, 1999 , vol. 40, # 5 p. 843 - 846
反应条件
hydrogen; Nic(w) in ethanol T=25°C; P=760 Torr; 11 h;
参考文献
Journal of Organic Chemistry, , vol. 45, # 10 p. 1946 - 1950
反应条件
sodium amalgam in methanol T=0°C; 0.5 h;
参考文献
Thompson, C. M.; Frick, J. A.; Woytowicz, C. E.
Synthetic Communications, 1988 , vol. 18, # 9 p. 889 - 892
反应条件
trichloromonobromomethane; Ir[(dF(CF3)ppy)2(dtbbpy)]PF6; water in acetonitrile 12 h; Inert atmosphereIrradiation;
参考文献
Tucker, Joseph W.; Narayanam, Jagan M. R.; Shah, Pinkey S.; Stephenson, Corey R. J.
Chemical Communications, 2011 , vol. 47, # 17 p. 5040 - 5042
反应条件
Fusarium fujikuroi in dimethyl sulfoxide T=28 - 30°C; 120 h; Microbiological reaction;
参考文献
Chemistry and Biodiversity, , vol. 10, # 10 p. 1909 - 1919
反应条件
ruthenium trichloride; sodium tetrahydroborate in N,N-dimethyl acetamide; water T=0°C; 1 h; chemoselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 2 p. 439 - 441
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=0°C; 0.5 h; Product distribution;
参考文献
Masaki, Yukio; Iwata, Ikuhiro; Mukai, Isao; Oda, Hirohisa; Nagashima, Hiromu
Chemistry Letters, 1989 , p. 659 - 662
反应条件
1: NaBH4 2: 60 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 107, # 18 p. 5225 - 5228
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 2: diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 44, # 22 p. 3888 - 3901
反应条件
1: (i) 9-bora-bicyclo<3.3.1>nonane, THF, (ii) aq. NaOH, H2O2 2: pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 3: diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 44, # 22 p. 3888 - 3901