6-甲基-5-庚烯-2-醇合成路线 （共 96 条）
反应条件
1: 74 percent / HBF4 / CH2Cl2; diethyl ether / 0.5 h / -30 °C 2: 10 N aq. NaOH / CH2Cl2; methanol / 24 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: KHSO4 / 0.75 h / 140 °C 2: 74 percent / HBF4 / CH2Cl2; diethyl ether / 0.5 h / -30 °C 3: 10 N aq. NaOH / CH2Cl2; methanol / 24 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: HBF4*Et2O / CH2Cl2 / -30 °C 2: methanol 3: t-BuOK / dimethylsulfoxide / 24 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 30 p. 4331 - 4334
反应条件
copper(l) iodide in tetrahydrofuran
参考文献
Tetrahedron Letters, , p. 4069 - 4072
反应条件
1: diisobutylaluminum hydride / tetrahydrofuran / 0.08 h / -78 °C 2: 86 percent / tetrahydrofuran / 1 h / 0 °C 3: 76 percent / 6percent sodium amalgam / methanol / 0.5 h / 0 °C View Scheme
参考文献
Synthetic Communications, , vol. 18, # 9 p. 889 - 892
反应条件
1: 86 percent / tetrahydrofuran / 1 h / 0 °C 2: 76 percent / 6percent sodium amalgam / methanol / 0.5 h / 0 °C View Scheme
参考文献
Synthetic Communications, , vol. 18, # 9 p. 889 - 892
反应条件
potassium hydrogensulfate T=140°C; 0.75 h; Yield given;
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
potassium carbonate im Autoklaven;
参考文献
Chemische Berichte, , vol. 31, p. 2989
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 126, p. 1423
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 128, p. 110
参考文献
Journal of Organic Chemistry, , vol. 44, # 22 p. 3888 - 3901
反应条件
copper(l) iodide; magnesium Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 27, # 34 p. 4079 - 4082
