6-甲基-5-庚烯-2-醇合成路线 （共 96 条）
反应条件
CAL-B in di-isopropyl ether T=30°C; Esterification; 5 h; Enzymatic reaction;
参考文献
Kita, Yasuyuki; Takebe, Yasushi; Murata, Kenji; Naka, Tadaatsu; Akai, Shuji
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 83 - 88
反应条件
porcine pancreatic lipase in diethyl ether 72 h; Ambient temperature;
参考文献
Stokes, Thomas M.; Oehlschlager, Allan C.
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2091 - 2094
反应条件
D-glucose; Yarrowia lipolytica YL10; peptone in N,N-dimethyl-formamide T=28°C; Oxidation; 72 h; Microbiological reaction; Title compound not separated from byproducts;
参考文献
Fantin, Giancarlo; Fogagnolo, Marco; Medici, Alessandro; Pedrini, Paola; Fontana, Silvia
Tetrahedron Asymmetry, 2000 , vol. 11, # 11 p. 2367 - 2373
反应条件
Lipase PS T=30°C; enantioselectivity of lipase PS on transesterification in various solvents; Rate constant;
参考文献
Steinreiber, Andreas; Stadler, Alexander; Mayer, Sandra F; Faber, Kurt; Kappe
Tetrahedron Letters, 2001 , vol. 42, # 36 p. 6283 - 6286
反应条件
lipase Amano PS enzyme in anhydrous butyl ether T=30°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Kita, Yasuyuki; Takebe, Yasushi; Murata, Kenji; Naka, Tadaatsu; Akai, Shuji
Tetrahedron Letters, 1996 , vol. 37, # 41 p. 7369 - 7372
反应条件
Candida antarctica lipase B T=35°C; P=350 Torr; Enzymatic reaction; enantioselective reaction;
参考文献
Monteiro, Carlos M.; Lourenco, Nuno M.T.; Afonso, Carlos A.M.
Tetrahedron Asymmetry, 2010 , vol. 21, # 8 p. 952 - 956
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
反应条件
porcine pancreatic lipase in diethyl ether 72 h; Ambient temperatureenantioselectivity of transesterification; Product distributionRate constant;
参考文献
Tetrahedron Letters, , vol. 28, # 19 p. 2091 - 2094
反应条件
Lipase PS; tert-butyl methyl ether T=30°C; Esterification; 20 h; Enzymatic reaction; Title compound not separated from byproducts.;
参考文献
Kita, Yasuyuki; Takebe, Yasushi; Murata, Kenji; Naka, Tadaatsu; Akai, Shuji
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 83 - 88
反应条件
alcohol dehydrogenase from Thermoanaerobium brockii; NADH-specific (R)-selective-ADH; YcnD-oxidoreductase T=30°C; pH=7.5; 6 h; aq. bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantiospecific reaction;
参考文献
Voss, Constance V.; Gruber, Christian C.; Faber, Kurt; Knaus, Tanja; Macheroux, Peter; Kroutil, Wolfgang
Journal of the American Chemical Society, 2008 , vol. 130, # 42 p. 13969 - 13972
