苯基-α-D-吡喃葡萄糖苷合成路线 （共 10 条）
反应条件
sodium methylate in methanol; dichloromethane
参考文献
Gridley, Jonathan J.; Hacking, Andrew J.; Osborn, Helen M. I.; Spackman, David G.
Tetrahedron, 1998 , vol. 54, # 49 p. 14925 - 14946
反应条件
sodium methylate in methanol 18 h;
参考文献
France, Robert R.; Compton, Richard G.; Davis, Benjamin G.; Fairbanks, Antony J.; Rees, Neil V.; Wadhawan, Jay D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 15 p. 2195 - 2202
反应条件
1: 89 percent / BF3*Et2O / CH2Cl2 / 48 h / 50 °C 2: 90 percent / MeONa / methanol / 18 h View Scheme
参考文献
France, Robert R.; Compton, Richard G.; Davis, Benjamin G.; Fairbanks, Antony J.; Rees, Neil V.; Wadhawan, Jay D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 15 p. 2195 - 2202
反应条件
1: 89 percent / BF3*Et2O / CH2Cl2 / 48 h / 50 °C 2: 90 percent / MeONa / methanol / 18 h View Scheme
参考文献
Hickinbottom
Journal of the Chemical Society, 1928 , p. 3140,3146
反应条件
1: Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin 2: NH3; ethanol View Scheme
参考文献
Hickinbottom
Journal of the Chemical Society, 1928 , p. 3140,3146
反应条件
1: benzene; ammonia 2: Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin 3: NH3; ethanol View Scheme
参考文献
Hickinbottom
Journal of the Chemical Society, 1928 , p. 3140,3146
反应条件
Xanthomonas campestris WU-9701 α-glucosyl transfer enzyme Enzymatic reaction; diastereoselective reaction;
参考文献
Sato, Toshiyuki; Hasegawa, Nobukazu; Saito, Jun; Umezawa, Satoru; Honda, Yuki; Kino, Kuniki; Kirimura, Kohtaro
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 80, p. 20 - 27
反应条件
2,6-dimethylpyridine T=100°C; nucleophilic selectivity and stereoselectivity; MechanismProduct distribution;
参考文献
Sinnott, Michael L.; Jencks, William P.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2026 - 2032
反应条件
trifluorormethanesulfonic acid T=100°C; nucleophilic selectivity and stereoselectivity; MechanismProduct distribution;
参考文献
Sinnott, Michael L.; Jencks, William P.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2026 - 2032
反应条件
Bacillus macerans cyclomaltodextrin glucanyltransferase in acidic aq. solution T=37°C; pH=6.0; 24 h; Further byproducts given;
参考文献
Yoon, Seung-Heon; Robyt, John F.
Carbohydrate Research, 2006 , vol. 341, # 2 p. 210 - 217
