反应条件
1: 1.) LDA / 1.) hexane, THF, -50 deg C, 30 min, 2.) hexamethylphosphoramide, -78 deg C, 1 h and room temperature, 4 h
2: 75 percent / LiAlH4 / diethyl ether / 1.) 0 deg C, 30 min, 2.) room temperature, overnight
View Scheme
参考文献
Madder, Annemieke; Sebastian, Sonny; Van Haver, Dirk; De Clercq, Pierre J.; Maskill, Howard
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 12 p. 2787 - 2793
