1-烯丙氧基-3-氯-2-丙醇合成路线 (共 10 条)
反应条件
1: 79 percent / KOH / diethyl ether / 2 h / 30 °C 2: 73 percent / thiourea; sulfuric acid / H2O / 1.5 h / 5 - 20 °C View Scheme
参考文献
Allakhverdiev; Askerov
Russian Journal of Applied Chemistry, 2003 , vol. 76, # 8 p. 1280 - 1283
反应条件
potassium hydroxide in diethyl ether T=30°C; 2 h;
参考文献
Allakhverdiev; Askerov
Russian Journal of Applied Chemistry, 2003 , vol. 76, # 8 p. 1280 - 1283
反应条件
ammonium cerium(IV) nitrate; tri-n-butyl benzyl ammonium chloride in acetonitrile
0.3 h; Ambient temperature;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Jamalian, Arezu
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 11 p. 2615 - 2621
反应条件
sulfuric acid; silica gel
T=20°C; 3.5 h;
参考文献
Salehi, Peyman; Dabiri, Minoo; Zolfigol, Mohammad Ali; Fard, Mohammad Ali Bodaghi
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 6 p. 1113 - 1121
反应条件
tetra-(n-butyl)-phosphonium bromide in diethylene glycol dimethyl ether
T=90°C; 12 h; shorter reaction time (-> primary addition product); other epoxides; Mechanism;
参考文献
Jin; Nishikubo
Tetrahedron Letters, 1992 , vol. 33, # 42 p. 6307 - 6308
反应条件
H3[PW12O40]
T=45°C; further epoxides and further alcohols; further heteropoly acid catalysts; Product distributionMechanism;
参考文献
Izumi, Yusuke; Hayashi, Kyoji
Chemistry Letters, 1980 , p. 787 - 790
反应条件
tin(IV) chloride
Rate constant;
参考文献
Drugov, M. V.; Barantsevich, E. N.; Smirnov P. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1052 - 1056
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1157 - 1162
参考文献
Pishnamazzade,B.F.; Mamishov,A.Kh.
Journal of Organic Chemistry USSR (English Translation), 1973 , vol. 9, p. 1394 - 1397
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, # 7 p. 1365 - 1369
反应条件
bromine in tetrachloromethane
参考文献
Kerimov; Orudzheva; Mamedova; Alieva
Russian Journal of Applied Chemistry, 2013 , vol. 86, # 9 p. 1364 - 1369
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), 2013 , vol. 86, # 9 p. 1394 - 1400,7
参考文献
Geigy A.G.
Patent: US2343053 , 1940 ;