3,3-二甲基-2-丁醇合成路线 （共 125 条）
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2] in methanol T=70°C; Leuckart-Wallach reaction; 30 h;
参考文献
Kitamura, Masato; Lee, Donghyun; Hayashi, Shinnosuke; Tanaka, Shinji; Yoshimura, Masahiro
Journal of Organic Chemistry, 2002 , vol. 67, # 24 p. 8685 - 8687
反应条件
D-glucopyranose; PFN; P450 BM3; oxygen in ethanol; N,N-dimethyl-formamide T=20°C; pH=8; 1 h; Inert atmosphereEnzymatic reaction; optical yield given as percent deregioselective reaction;
参考文献
Zilly, Felipe E.; Acevedo, Juan P.; Augustyniak, Wojciech; Deege, Alfred; Reetz, Manfred T.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 12 p. 2720 - 2724
参考文献
Conant; Blatt
Journal of the American Chemical Society, 1929 , vol. 51, p. 1233
参考文献
Conant; Blatt
Journal of the American Chemical Society, 1929 , vol. 51, p. 1233
反应条件
1,1,2,2-tetramethylethylene
参考文献
Snider; Rodini; Kirk; Cordova
Journal of the American Chemical Society, 1982 , vol. 104, # 2 p. 555 - 563
反应条件
tetra-n-butylammonium nitridoosmate(VIII); iron(III) chloride in dichloromethane; acetic acid T=23°C; 0.00833333 h; Product distribution; Further Variations:ReagentsTemperaturesSolventstime;
参考文献
Yiu, Shek-Man; Wu, Zhi-Biao; Mak, Chi-Keung; Lau, Tai-Chu
Journal of the American Chemical Society, 2004 , vol. 126, # 45 p. 14921 - 14929
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) 12 h; Ambient temperature; Yields of byproduct given;
参考文献
Menicagli, Rita; Malanga, Corrado; Finato, Barbara; Lardicci, Luciano
Gazzetta Chimica Italiana, 1989 , vol. 119, # 1 p. 69 - 70
反应条件
in ethanol; water 72 h; Mortierella isabellina NRRL 1757;
参考文献
Holland, Herbert L.; Munoz, Benito
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2299 - 2303
反应条件
1: 1.) n-butyllithium / 1.) THF, 0 deg C, 30 min; 2.) -78 deg C, 2 h 2: 74 percent / potassium tert-butoxide / H2O; dimethylsulfoxide / 48 h / Ambient temperature View Scheme
参考文献
Larson, Gerald L.; Prieto, J. Antonio; Ortiz, Edgardo
Tetrahedron, 1988 , vol. 44, # 13 p. 3781 - 3790
反应条件
1: ruthenium / water / 24 h / 60 °C / |Sealed tube; |Inert atmosphere 2: Rh(1+)*C7H8*C42H46O3P2*BF4(1-); hydrogen / dichloromethane / 24 h / 40 °C / 3000.3 Torr / |Glovebox; |Inert atmosphere 3: potassium carbonate; methanol View Scheme
参考文献
Kleman, Patryk; Gonzalez-Liste, Pedro J.; Garcia-Garrido, Sergio E.; Cadierno, Victorio; Pizzano, Antonio
Chemistry - A European Journal, 2013 , vol. 19, # 48 p. 16209 - 16212
