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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
樟脑
合成路线
（共 212 条）
64031-55-6
→
反应条件
464-49-3
樟脑
反应条件
1.1: N-ethyl-N,N-diisopropylamine; (1,2-dibromo-1-phenyl-ethyl)-phosphonic acid / dichloromethane / 24 h / 20 °C 1.2: 24 h / 20 °C 2.1: Streptomyces coelicolor A3(2) 2-methylisoborneol synthase; magnesium chloride; sodium chloride; 2-hydroxyethanethiol / aq. buffer / 12 h / 30 °C / pH 7 / |Enzymatic reaction View Scheme
参考文献
Koeksal, Mustafa; Chou, Wayne K. W.; Cane, David E.; Christianson, David W.
Biochemistry, 2013 , vol. 52, # 31 p. 5247 - 5255
1841-92-5
→
反应条件
464-49-3
樟脑
反应条件
1.1: diisobutylaluminium hydride / toluene / 12 h / 20 °C 2.1: triethylamine / dichloromethane / 1 h / 0 °C 3.1: 2,4,6-trimethyl-pyridine; water / acetone / 3 h / 60 °C 4.1: N-ethyl-N,N-diisopropylamine; (1,2-dibromo-1-phenyl-ethyl)-phosphonic acid / dichloromethane / 24 h / 20 °C 4.2: 24 h / 20 °C 5.1: Streptomyces coelicolor A3(2) 2-methylisoborneol synthase; magnesium chloride; sodium chloride; 2-hydroxyethanethiol / aq. buffer / 12 h / 30 °C / pH 7 / |Enzymatic reaction View Scheme
参考文献
Koeksal, Mustafa; Chou, Wayne K. W.; Cane, David E.; Christianson, David W.
Biochemistry, 2013 , vol. 52, # 31 p. 5247 - 5255
2284-91-5
→
反应条件
464-49-3
樟脑
反应条件
1.1: triethylamine / dichloromethane / 1 h / 0 °C 2.1: 2,4,6-trimethyl-pyridine; water / acetone / 3 h / 60 °C 3.1: N-ethyl-N,N-diisopropylamine; (1,2-dibromo-1-phenyl-ethyl)-phosphonic acid / dichloromethane / 24 h / 20 °C 3.2: 24 h / 20 °C 4.1: Streptomyces coelicolor A3(2) 2-methylisoborneol synthase; magnesium chloride; sodium chloride; 2-hydroxyethanethiol / aq. buffer / 12 h / 30 °C / pH 7 / |Enzymatic reaction View Scheme
参考文献
Koeksal, Mustafa; Chou, Wayne K. W.; Cane, David E.; Christianson, David W.
Biochemistry, 2013 , vol. 52, # 31 p. 5247 - 5255
15099-93-1
2-去氢樟脑
→
反应条件
464-49-3
樟脑
反应条件
palladium on activated charcoal; acetic acid Hydrogenation;
参考文献
Maelkoenen
Annales Academiae Scientiarum Fennicae, Series A2: Chemica, 1964 , # 128 p. 30,41
2792-42-9
(1R)-樟脑肟
→
反应条件
464-49-3
樟脑
+
26585-74-0
[(1R)-2,2,3-三甲基-3-环戊烯-1-基]乙腈
+
113375-34-1
+
108268-00-4
反应条件
in methanol T=20 - 30°C; 15 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Suginome, Hiroshi; Furukawa, Kenji; Orito, Kazuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 4 p. 917 - 921
2792-42-9
(1R)-樟脑肟
→
反应条件
464-49-3
樟脑
+
26585-74-0
[(1R)-2,2,3-三甲基-3-环戊烯-1-基]乙腈
+
113375-34-1
+
107133-28-8
反应条件
in methanol T=20 - 30°C; 15 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Suginome, Hiroshi; Furukawa, Kenji; Orito, Kazuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 4 p. 917 - 921
60300-67-6
→
反应条件
464-49-3
樟脑
+
129594-73-6
+
100-52-7
苯甲醛
反应条件
lithium diisopropyl amide in tetrahydrofuran Ambient temperature3-4 h;
参考文献
Hutchinson, J. H.; Li, D. L. F.; Money, T.; Palme, M.; Agharahimi, M. R.; Albizati, K. F.
Canadian Journal of Chemistry, 1991 , vol. 69, # 3 p. 558 - 566
14487-70-8
→
反应条件
464-49-3
樟脑
反应条件
sodium dithionite; diethyl ether; tin(ll) chloride
参考文献
Forster; Saville
Journal of the Chemical Society, 1920 , vol. 117, p. 759
464-17-5
1,7,7-三甲雙環[2.2.1]庚-2-烯
→
反应条件
464-49-3
樟脑
+
10292-98-5
反应条件
potassium permanganate; sodium amalgam; mercury(II) diacetate 1)acetic acid,room temp.;2)ether;; Multistep reaction;
参考文献
Skorobogatova, E. V.; Povelikina, L. N.; Kartashov, V. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1979 - 1982
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 11 p. 2318 - 2321
30462-53-4
→
反应条件
464-49-3
樟脑
反应条件
1: 50 percent / Potassium cyclohexyl oxide / 10 h / Heating; Cyclohexanol as solvent 2: 1)mercuric acetate 2)sodium amalgam 3)potassium permanganate / 1)acetic acid,room temp.;2)ether; View Scheme
参考文献
Skorobogatova, E. V.; Povelikina, L. N.; Kartashov, V. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1979 - 1982
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 11 p. 2318 - 2321
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