反应条件
1: 90 percent / HgO; conc. H2SO4 / acetone; H2O / 0.25 h / 60 °C 2: 99 percent / KH / tetrahydrofuran; various solvent(s) / 1 h / 20 °C 3: 94 percent / LDA / tetrahydrofuran; hexane / 0.25 h / -78 °C 4: 98 percent / H2 / Pd/C / ethyl acetate / 1 h / 20 °C 5: 95 percent / EDC; HOBT / CH2Cl2 / 17 h / 0 - 20 °C 6: TBAF / tetrahydrofuran / 0.33 h / 20 °C 7: aq. cerium ammonium nitrate / acetonitrile / 0.08 h / 20 °C View Scheme
参考文献
Palomo, Claudio; Oiarbide, Mikel; Aizpurua, Jesus M.; Gonzalez, Alberto; Garcia, Jesus M.; Landa, Cristina; Odriozola, Ibon; Linden, Anthony
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8193 - 8200
