(4-溴苯基)(2-氯苯基)甲酮合成路线 (共 5 条)
反应条件
copper ferrite in neat (no solvent) T=80°C; Friedel-Crafts Acylation; 24 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=0°C; 10 h;
参考文献
Yoshida, Hiroto; Mimura, Yasuhiro; Ohshita, Joji; Kunai, Atsutaka
Chemical Communications, 2007 , # 23 p. 2405 - 2407
反应条件
chromium(VI) oxide; sulfuric acid in acetone T=20°C; Jones oxidation; 0.166667 h;
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.08 h / -78 °C 1.2: tetrahydrofuran 2.1: CrO3; H2SO4 / acetone / 0.17 h / 20 °C View Scheme
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.08 h / -78 °C 1.2: tetrahydrofuran 2.1: CrO3; H2SO4 / acetone / 0.17 h / 20 °C View Scheme
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605