3-(4-氟苯基)-5-甲基-4-异恶唑羰酰氯合成路线 （共 4 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane
1 h; Heating;
参考文献
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228
反应条件
1: 38 percent / Et3N / diethyl ether / 0.75 h
2: conc. aq. HCl, CH3COOH / 72 h / Heating
3: oxalyl chloride, DMF / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228
反应条件
1: N-chlorosuccinimide / dimethylformamide / Ambient temperature
2: 38 percent / Et3N / diethyl ether / 0.75 h
3: conc. aq. HCl, CH3COOH / 72 h / Heating
4: oxalyl chloride, DMF / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228
反应条件
1: conc. aq. HCl, CH3COOH / 72 h / Heating
2: oxalyl chloride, DMF / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228
