2,3,4-三甲氧基-beta-硝基苯乙烯合成路线 （共 2 条）
反应条件
ammonium acetate; acetic acid
T=100°C; 12 h;
参考文献
Yang, Su Hui; Song, Chin-Hee; Van, Hue Thi My; Park, Eunsook; Khadka, Daulat Bikram; Gong, Eun-Yeung; Lee, Keesook; Cho, Won-Jea
Journal of Medicinal Chemistry, 2013 , vol. 56, # 8 p. 3414 - 3418
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 80 °C
2: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C
3: poly-phosphoric acid / 0.17 h / 145 °C
4: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / |Reflux
View Scheme
参考文献
Yang, Su Hui; Song, Chin-Hee; Van, Hue Thi My; Park, Eunsook; Khadka, Daulat Bikram; Gong, Eun-Yeung; Lee, Keesook; Cho, Won-Jea
Journal of Medicinal Chemistry, 2013 , vol. 56, # 8 p. 3414 - 3418
