(9CI)-[(5-乙基-3-噻吩)乙炔]三甲基-硅烷合成路线 （共 3 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine
T=75°C; Sonogashira reaction;
参考文献
Aso, Yoshio; Obara, Yuko; Okai, Takashi; Nishiguchi, Shoji; Otsubo, Tetsuo
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 376, p. 153 - 158
反应条件
1: 95 percent / diethyl ether / 20 °C
2: 91 percent / TMSCl; NaI / acetonitrile; hexane / 20 °C
3: 97 percent / Pd(PPh3)4; CuI; Et3N / 75 °C
View Scheme
参考文献
Aso, Yoshio; Obara, Yuko; Okai, Takashi; Nishiguchi, Shoji; Otsubo, Tetsuo
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 376, p. 153 - 158
反应条件
1: 91 percent / TMSCl; NaI / acetonitrile; hexane / 20 °C
2: 97 percent / Pd(PPh3)4; CuI; Et3N / 75 °C
View Scheme
参考文献
Aso, Yoshio; Obara, Yuko; Okai, Takashi; Nishiguchi, Shoji; Otsubo, Tetsuo
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 376, p. 153 - 158
