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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
(+)-香柏酮
合成路线
（共 28 条）
72453-44-2
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
sodium acetate in water; acetic acid T=100°C; 2 h;
参考文献
Sauer, Anne M.; Crowe, William E.; Henderson, Gregg; Laine, Roger A.
Organic Letters, 2009 , vol. 11, # 16 p. 3530 - 3533
10219-75-7
佛术烯
→
反应条件
136918-14-4
+
4674-50-4
(+)-香柏酮
+
840474-83-1
反应条件
oxygen; 2-hydroxy-1,3-isoindolinedione; cobalt nitrate; anhydrous cobalt diacetate; Co(acac)3 in acetonitrile T=40°C; P=9750.98 Torr; 3 h; Product distribution / selectivity;
参考文献
Sugahara, Michihiro
Patent: US2004/14985 A1, 2004 ;
Location in patent: Page 9 ;
10219-75-7
佛术烯
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
Czapek-pepton medium; Pallavicinia subcilita T=30°C; pH=7.0; 168 h;
参考文献
Furusawa, Mai; Hashimoto, Toshihiro; Noma, Yoshiaki; Asakawa, Yoshinori
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 11 p. 1513 - 1514
72453-44-2
→
反应条件
15764-04-2
4,4A,5,6,7,8-六氢-4,4A-二甲基-6-(1-甲基亚乙基)-(4R-顺)-2(3H)-萘酮
+
4674-50-4
(+)-香柏酮
反应条件
aluminum oxide in hexane T=60°C; 24 h;
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
38651-65-9
(1R)-(+)-诺蒎酮
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: 88 percent / triethylamine / dimethylformamide / 24 h / 95 °C 2: 96 percent / TiCl4 / CH2Cl2 / 1.5 h / -78 °C 3: 90 percent / p-toluenesulfonic acid / benzene / 2 h / Heating 4: 81 percent / TiCl4 / CH2Cl2 5: 71 percent / NaNH2 / benzene 6: 1.) O3; 2.) Zn/CH3COOH / 1.) -78 deg C, 30 min; 2.) room temperature overnight. 7: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 8: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
72453-38-4
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: 90 percent / p-toluenesulfonic acid / benzene / 2 h / Heating 2: 81 percent / TiCl4 / CH2Cl2 3: 71 percent / NaNH2 / benzene 4: 1.) O3; 2.) Zn/CH3COOH / 1.) -78 deg C, 30 min; 2.) room temperature overnight. 5: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 6: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
72453-33-9
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: 96 percent / TiCl4 / CH2Cl2 / 1.5 h / -78 °C 2: 90 percent / p-toluenesulfonic acid / benzene / 2 h / Heating 3: 81 percent / TiCl4 / CH2Cl2 4: 71 percent / NaNH2 / benzene 5: 1.) O3; 2.) Zn/CH3COOH / 1.) -78 deg C, 30 min; 2.) room temperature overnight. 6: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 7: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
73068-31-2
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: p-toluenesulfonic acid monohydrate / ethanol / 3 h / Ambient temperature 2: 81 percent / TiCl4 / CH2Cl2 3: 71 percent / NaNH2 / benzene 4: 1.) O3; 2.) Zn/CH3COOH / 1.) -78 deg C, 30 min; 2.) room temperature overnight. 5: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 6: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
72453-37-3
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: 81 percent / TiCl4 / CH2Cl2 2: 71 percent / NaNH2 / benzene 3: 1.) O3; 2.) Zn/CH3COOH / 1.) -78 deg C, 30 min; 2.) room temperature overnight. 4: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 5: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
72453-41-9
→
反应条件
4674-50-4
(+)-香柏酮
反应条件
1: 73 percent / HCl / acetic acid / 21 h / Ambient temperature 2: Al2O3 / hexane / 24 h / 60 °C View Scheme
参考文献
Yanami, Tetsuji; Miyashita, Masaaki; Yoshikoshi, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 607 - 612
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