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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
468060-75-5
合成路线
（共 7 条）
88952-72-1
→
反应条件
468060-75-5
反应条件
boron tribromide in dichloromethane T=-78 - 20°C; 18 h;
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
106-44-5
对甲酚
→
反应条件
468060-75-5
反应条件
1: pyridine 2: AlCl3 3: 91 percent / pyridine / 0.5 h / 50 °C 4: 85 percent / pyridine; KOH / 1.5 h / 50 °C 5: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 6: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
1450-72-2
2-羟基-5-甲基苯乙酮
→
反应条件
468060-75-5
反应条件
1: 91 percent / pyridine / 0.5 h / 50 °C 2: 85 percent / pyridine; KOH / 1.5 h / 50 °C 3: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 4: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
468060-75-5
反应条件
1: AlCl3 2: 91 percent / pyridine / 0.5 h / 50 °C 3: 85 percent / pyridine; KOH / 1.5 h / 50 °C 4: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 5: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
1711-05-3
间甲氧基苯甲酰氯
→
反应条件
468060-75-5
反应条件
1: 91 percent / pyridine / 0.5 h / 50 °C 2: 85 percent / pyridine; KOH / 1.5 h / 50 °C 3: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 4: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
88951-98-8
→
反应条件
468060-75-5
反应条件
1: 85 percent / pyridine; KOH / 1.5 h / 50 °C 2: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 3: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
88952-35-6
→
反应条件
468060-75-5
反应条件
1: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 2: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
