4-[2-(3-硝基苯基)乙烯基]吡啶合成路线 （共 7 条）
反应条件
in nitrobenzene T=30°C; other temperatures; Ea, ΔH(excit.), ΔS(excit.), log PZ; Rate constantThermodynamic data;
参考文献
Ananthakrishnanadar, P.; Rajasekaran, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 324 - 325
反应条件
1: With SnCl2·2H2O; ethanol T=60°C; 16 h; Inert atmosphere; 2: With sodium hydroxide in water; ethyl acetate Product distribution / selectivity;
参考文献
Société Splicos; Centre National de la Recherche Scientifique; Institut Curie; Université de Montpellier 2
Patent: EP2505198 A1, 2012 ;
Location in patent: Page/Page column 44 ;
反应条件
sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide
T=135°C; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Société Splicos; Centre National de la Recherche Scientifique; Institut Curie; Université de Montpellier 2
Patent: EP2505198 A1, 2012 ;
Location in patent: Page/Page column 44 ;
反应条件
TEA; palladium diacetate in acetonitrile
T=100°C; 48 h;
参考文献
Bramson; Holmes; Hunter; Lackey; Lovejoy; Luzzio; Montana; Rocque; Rusnak; Shewchuk; Veal; Corona; Walker; Kuyper; Davis; Dickerson; Edelstein; Frye; Gampe Jr.; Harris; Hassell
Journal of Medicinal Chemistry, 2001 , vol. 44, # 25 p. 4339 - 4358
反应条件
bis(acetylacetonato) palladium; oxygen; sodium hydrogencarbonate in N,N-dimethyl-formamide
T=90°C; Heck reaction; P=760.051 Torr; 24 h;
参考文献
Shi, Chuanli; Ding, Jinchang; Jiang, Jun; Chen, Jiuxi; Wu, Huayue; Liu, Miaochang
Journal of Chemical Research, 2012 , vol. 36, # 6 p. 322 - 325
参考文献
Wagstaff
Journal of the Chemical Society, 1934 , p. 276
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Horwitz
Journal of Organic Chemistry, 1956 , vol. 21, p. 1039
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Michaillow; Ter-Sarkisjan
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1954 , p. 846,851;engl.Ausg. 731,735
参考文献
Michaillow; Ter-Sarkisjan
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1954 , p. 846,851;engl.Ausg. 731,735
