2,2-二苯基-乙酰苯胺合成路线 (共 50 条)
反应条件
lithium perchlorate in water; acetonitrile Electrolysis;
参考文献
Golub, Tatiana; Becker, James Y.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 19 p. 3906 - 3912
反应条件
in tetrahydrofuran added at 0 deg C, then 20 deg C;
参考文献
Kolodyazhnyi, O. I.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1314 - 1318,1156 - 1159
反应条件
bromine; triethylamine; triphenylphosphine in dichloromethane Heating;
参考文献
Bestmann,H.J. et al.
Justus Liebigs Annalen der Chemie, 1968 , vol. 718, p. 24 - 32
反应条件
Me2NH*BH3; potassium carbonate; triphenylphosphine; NiCl2((PPh3)P)2 in acetonitrile
T=40°C; 12 h;
参考文献
Lipshutz, Bruce H.; Tomioka, Takashi; Pfeiffer, Steven S.
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7737 - 7740
反应条件
triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
T=20°C; 0.0166667 h; chemoselective reaction;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Nowrouzi, Najmeh; Khalili, Dariush
Tetrahedron, 2009 , vol. 65, # 19 p. 3893 - 3899
反应条件
1: N'-(diphenylmethylene)-4-methylbenzene-1-sulfonohydrazide With sodium hydride in toluene; mineral oil
T=0 - 20°C; 0.5 h; Inert atmosphere;
2: carbon monoxide; aniline With tris-(dibenzylideneacetone)dipalladium(0); Aliquat® 336; potassium carbonate in toluene; mineral oil
T=60°C; P=760.051 Torr; 96 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
反应条件
tetraethylammonium tetrafluoroborate in dichloromethane
anodic oxidation at the first oxidation wave, Pt anode, 0.42 F/mol;
参考文献
Becker, James Y.; Shakkour, Elias; Sarma, J. A. P. R.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3716 - 3720
反应条件
in tetrahydrofuran
T=20°C; 4 h;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane; water
24 h; Inert atmosphereReflux;
参考文献
Ye, Wenchao; Mo, Jun; Zhao, Tiankun; Xu, Bin
Chemical Communications, 2009 , # 22 p. 3246 - 3248
反应条件
InI3
T=110 - 120°C; 9 h;
参考文献
Ranu, Brindaban C.; Dutta, Pinak
Synthetic Communications, 2003 , vol. 33, # 2 p. 297 - 301