2,2-二苯基-乙酰苯胺合成路线 (共 50 条)
反应条件
1: sodium carbonate / H2O / 1.5 h / 55 - 60 °C / nonionic tenside
2: 97 percent / 1.) aq. NaNO2, sodium laurylosulphonate, 2.) aq. H2SO4
View Scheme
参考文献
Eckstein, Z.; Jelenski, P.; Kowal, J.; Rusek, D.
Synthetic Communications, 1982 , vol. 12, # 3 p. 201 - 208
反应条件
1: sodium carbonate / H2O / 1.5 h / 55 - 60 °C / nonionic tenside
2: 97 percent / 1.) aq. NaNO2, sodium laurylosulphonate, 2.) aq. H2SO4
View Scheme
参考文献
Eckstein, Z.; Jelenski, P.; Kowal, J.; Rusek, D.
Synthetic Communications, 1982 , vol. 12, # 3 p. 201 - 208
反应条件
chloro(phenylmethyl)-magnesium in tetrahydrofuran; benzene
参考文献
Flitsch,W.; Heidhues,R.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1966 , vol. 21b, p. 1137 - 1141
反应条件
potassium hydroxide in ethanol
参考文献
Rigaudy,J. et al.
Bulletin de la Societe Chimique de France, 1969 , p. 2756 - 2764
反应条件
1: benzene
2: concentrated hydrochloric acid
View Scheme
参考文献
Staudinger; Meyer
Chemische Berichte, 1920 , vol. 53, p. 76
反应条件
in ethylene glycol dimethyl ether
Heating;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1431 - 1435
参考文献
Klingemann
Justus Liebigs Annalen der Chemie, 1893 , vol. 275, p. 84
反应条件
hydrogenchloride; sodium nitrite
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1924 , vol. 43, p. 853
反应条件
1: PCl5
2: diethyl ether
View Scheme
参考文献
Klingemann
Justus Liebigs Annalen der Chemie, 1893 , vol. 275, p. 84
反应条件
1: benzene
2: concentrated hydrochloric acid
View Scheme
参考文献
Staudinger; Meyer
Chemische Berichte, 1920 , vol. 53, p. 76