3,5,5-三甲基-2-环己烯-1-醇合成路线 （共 27 条）
反应条件
18-crown-6 ether; tert-butylamine; tert-butyl alcohol; potassium in tetrahydrofuran T=20°C; 3 h;
参考文献
Shi, Lei; Wu, Jiong Xia; Fu, Min Zhang; Yong, Qiang Tu
Synlett, 2002 , # 9 p. 1505 - 1507
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 6 h;
参考文献
Winska; Wawrzenczyk
Polish Journal of Chemistry, 2007 , vol. 81, # 11 p. 1887 - 1897
反应条件
ATPH; n-butyllithium; diisobutylaluminium hydride in toluene T=-78 - 25°C; 0.25 h; Yields of byproduct given;
参考文献
Saito, Susumu; Yamamoto, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 9 p. 2928 - 2929
反应条件
sodium tetrahydroborate; N-hexadecyl-N,N-bis(2-hydroxyethyl)-N-methylammonium bromide in water; toluene T=20°C; 20 h; Yields of byproduct given;
参考文献
D'Incan, E.; Loupy, A.
Tetrahedron, 1981 , vol. 37, p. 1171 - 1180
反应条件
ATPH; n-butyllithium; diisobutylaluminium hydride 1) toluene, -78 deg C; 2) toluene, THF, hexane, -78 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Loupy, Andre; Seyden-Penne, Jacqueline
Tetrahedron, 1980 , vol. 36, p. 1937 - 1942
反应条件
[Cu(PPh3)2NO3]; hydrogen; (2S, 4S)-(-)-2,4-bis(diphenylphosphino)pentane; sodium t-butanolate in isopropyl alcohol T=30°C; P=37503.8 Torr; 18 h; enantioselective reaction;
参考文献
Shimizu, Hideo; Nagano, Takuto; Sayo, Noboru; Saito, Takao; Ohshima, Takashi; Mashima, Kazushi
Synlett, 2009 , # 19 p. 3143 - 3146
反应条件
zinc-modified cyanobrohydride in diethyl ether 6 h; Ambient temperature; Yield given;
参考文献
Kim, Kwan Eung; Park, Soo Bong; Yoon, Nung Min
Synthetic Communications, 1988 , vol. 18, # 1 p. 89 - 96
反应条件
cobalt nanoparticles in tetrahydrofuran T=66°C; 10 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Nador, Fabiana; Mascaro, Evangelina; Castro, Melisa; Vitale, Cristian; Radivoy, Gabriel
Arkivoc, 2011 , vol. 2011, # 7 p. 312 - 326
反应条件
Li(1+)*C12H28AlO3(1-) in tetrahydrofuran; hexane T=-78°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Geribaldi, Serge; Decouzon, Michele; Boyer, Bernard; Moreau, Claude
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1327 - 1330
反应条件
isopropyl alcohol Isolierung ueber das Benzoyl-Derivat;
参考文献
Kharasch; Tawney
Journal of the American Chemical Society, 1941 , vol. 63, p. 2308,2313
Journal of the American Chemical Society, 1945 , vol. 67, p. 128,130
