3,5,5-三甲基-2-环己烯-1-醇合成路线 （共 27 条）
反应条件
sodium tetrahydroborate; amphiphilic carbohydrate in water 12 h; Ambient temperature;
参考文献
Denis, Cecile; Laignel, Benoit; Plusquellec, Daniel; Le Marouille, Jean-Yves; Botrel, Alain
Tetrahedron Letters, 1996 , vol. 37, # 1 p. 53 - 56
反应条件
ATPH; n-butyllithium; diisobutylaluminium hydride 1) toluene, -78 deg C; 2) toluene, THF, hexane, -78 deg C --> rt; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Saito, Susumu; Yamamoto, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 9 p. 2928 - 2929
反应条件
sodium hydroxide; sodium tetrahydroborate in water T=14.9°C; with and without var. hydrotropes; other temp.; Product distribution;
参考文献
D'Incan, E.; Loupy, A.
Tetrahedron, 1981 , vol. 37, p. 1171 - 1180
反应条件
propionic acid T=140°C;
参考文献
Jones, Graham B.; Huber, Robert S.; Chau, Sotheary
Tetrahedron, 1993 , vol. 49, # 2 p. 369 - 380
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium tert-butylate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 2,4-dichlorotoluene T=25°C; 2 h; Inert atmosphere;
参考文献
Berini, Christophe; Winkelmann, Ole H.; Otten, Jennifer; Vicic, David A.; Navarro, Oscar
Chemistry - A European Journal, 2010 , vol. 16, # 23 p. 6857 - 6860
反应条件
α-L-Ara; dihydrogen peroxide; molibdic acid in phosphate buffer T=2°C; pH=7; 24 h; Product distribution; Further Variations:CatalystsReagentstime;
参考文献
Denis; Misbahi; Kerbal; Ferrieres; Plusquellec
Chemical Communications, 2001 , # 23 p. 2460 - 2461
反应条件
3,3-dimethyldioxirane in tetrachloromethane; acetone 12 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Adam, Waldemar; Smerz, Alexander K.
Tetrahedron, 1995 , vol. 51, # 47 p. 13039 - 13044
反应条件
1: With mercury(II) diacetate 18 h; Heating; 2: T=215°C; Claisen rearrangement; 0.75 h;
参考文献
Alameda-Angulo, Celia; Quiclet-Sire, Beatrice; Zard, Samir Z.
Tetrahedron Letters, 2006 , vol. 47, # 6 p. 913 - 916
反应条件
1: 77 percent / mercuric acetate , allyl alcohol / 24 h / 33 °C 2: 75 percent / 0.5 h / 215 °C View Scheme
参考文献
Boivin, Jean; Fouquet, Eric; Zard, Samir Z.
Tetrahedron Letters, 1990 , vol. 31, # 1 p. 85 - 88
反应条件
N-bromosuccinmide in dichloromethane T=-20°C;
参考文献
Srikrishna; Viswajanani; Yelamaggad
Tetrahedron, 1997 , vol. 53, # 30 p. 10479 - 10488
