N-(2,6-二甲基苯基)-4-甲酸苯磺酰胺合成路线 （共 11 条）
反应条件
naphthalene; water; lithium 1.) THF, -78 deg C - 20 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1997 , vol. 53, # 42 p. 14355 - 14368
反应条件
1: 74 percent / conc. HNO3 / acetic acid; H2O / 4 h / 140 °C 2: 64 percent / aq. H2SO4 / 16 h / 40 °C View Scheme
参考文献
Leffek, Kenneth T.; Pruszynski, Przemyslaw
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1454 - 1458
反应条件
(Na1752K0.144Ca0365Mg0.065)(Al2044Si2774O96)*19.16H2O in ethanol
T=25 - 30°C; 0.333333 h; SonicationGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Ehsani, Ali; Rostami-Vartouni, Akbar
Ultrasonics Sonochemistry, 2014 , vol. 21, # 1 p. 275 - 282
反应条件
potassium carbonate in water
7 h; Reflux;
参考文献
Azarifar, Davood; Soleimanei, Fatemeh
RSC Advances, 2014 , vol. 4, # 24 p. 12119 - 12126
反应条件
[(tris(3,5-dimethylpyrazol-1-yl)methane)Fe(NCMe)3](BF4)2 in dichloromethane
T=19.84°C; Overall yield = 74 percent; regioselective reaction;
参考文献
Liang, Shengwen; Jensen, Michael P.
Organometallics, 2012 , vol. 31, # 23 p. 8055 - 8058
反应条件
1: cyanic acid sodium salt / water / 0.17 h / |Reflux
2: potassium carbonate / water / 7 h / |Reflux
View Scheme
参考文献
Azarifar, Davood; Soleimanei, Fatemeh
RSC Advances, 2014 , vol. 4, # 24 p. 12119 - 12126
反应条件
1: 100 percent / sodium hydrogentelluide (NaTeH) / ethanol; diethyl ether / 0.25 h / Ambient temperature
2: tosylation
View Scheme
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
反应条件
in tetrahydrofuran; water
0.5 h;
参考文献
Rahaim Jr., Ronald J.; Maleczka Jr., Robert E.
Synthesis, 2006 , # 19 p. 3316 - 3340
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
反应条件
nitric acid; sodium nitrite in water; acetic acid
Reflux;
参考文献
Moorthy, Jarugu Narasimha; Saha, Satajit
European Journal of Organic Chemistry, 2009 , # 5 p. 739 - 748
