4-甲基-N,N-二苯基-苯磺酰胺合成路线 （共 17 条）
反应条件
1: With Na/K absorbed into silica gel in tetrahydrofuran T=20°C; Inert atmosphere; 2: With water in tetrahydrofuran
参考文献
Nandi, Partha; Redko, Mikhail Y.; Petersen, Kathryn; Dye, James L.; Lefenfeld, Michael; Vogt, Paul F.; Jackson, James E.
Organic Letters, 2008 , vol. 10, # 23 p. 5441 - 5444
反应条件
1: 1-methyl-2,3-indolinedione With sodium amalgam in N,N-dimethyl-formamide T=20°C; 4 h; 2: Ph2NTs in N,N-dimethyl-formamide T=110°C; 18 h;
参考文献
Sword, Ryan; O'Sullivan, Steven; Murphy, John A.
Australian Journal of Chemistry, 2013 , vol. 66, # 3 p. 314 - 322
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 1 h, 2.) room temp., 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hellwinkel, D.; Karle, R.
Synthesis, 1989 , # 5 p. 394 - 395
反应条件
in diethyl ether Ambient temperatureIrradiationvar. solvents; Product distributionMechanism;
参考文献
Angewandte Chemie, , vol. 92, # 8 p. 647 - 649
参考文献
Halberkann
Chemische Berichte, 1922 , vol. 55, p. 3083
反应条件
aluminum oxide; cesium fluoride in N,N-dimethyl-formamide 4 h; Heating;
参考文献
Hellwinkel; Goke
Synthesis, 1995 , # 9 p. 1135 - 1141
反应条件
(Na1752K0.144Ca0365Mg0.065)(Al2044Si2774O96)*19.16H2O in ethanol
T=25 - 30°C; 0.533333 h; SonicationGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Ehsani, Ali; Rostami-Vartouni, Akbar
Ultrasonics Sonochemistry, 2014 , vol. 21, # 1 p. 275 - 282
反应条件
cesium fluoride in acetonitrile
T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
1: iodyl sulfate; acetic acid anhydride; H2SO4 / anschl. mit wss. NaBr
2: aq. NaOH solution; benzene
View Scheme
参考文献
Beringer et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2705,2707
Journal of the American Chemical Society, 1959 , vol. 81, p. 342,346
反应条件
sodium hydroxide; benzene
参考文献
Beringer et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2705,2707
Journal of the American Chemical Society, 1959 , vol. 81, p. 342,346
