3-(2-呋喃甲基)-2-亚磺酰基噻唑烷-4-酮合成路线 (共 4 条)
反应条件
potassium carbonate in water
12 h; Reflux;
参考文献
Kamila, Sukanta; Ankati, Haribabu; Harry, Emily; Biehl, Edward R.
Tetrahedron Letters, 2012 , vol. 53, # 17 p. 2195 - 2198
反应条件
1: furan-2-ylmethylamine With cyanomethide anion in acetonitrile
T=-20°C; 1 h;
2: carbon disulfide in acetonitrile
T=-20°C; 1 h;
3: ethyl bromoacetate in acetonitrile
T=-20 - 20°C;
参考文献
Tissaoui, Khalil; Raouafi, Noureddine; Boujlel, Khaled
Journal of Sulfur Chemistry, 2010 , vol. 31, # 1 p. 41 - 48
反应条件
ammonium hydroxide; sodium hydroxide
anschliessendes Erwaermen mit wss. HCl;
参考文献
Brown et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 384,388
反应条件
triethylamine in water; acetone
0.5 h;
参考文献
Krus, K.; Masias, A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 10 p. 1824 - 1825
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 10 p. 2024 - 2026