molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in dichloromethane T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Palomo, Claudio; Aizpurua, Jesus M.; Garcia, Jesus M.; Ganboa, Inaki; Cossio, F. P.; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2498 - 2503
1: (benzyl)-triphenylphosphonium chloride With n-butyllithium in tetrahydrofuran; hexane T=0°C; Wittig type reaction; 2: (4-methylphenyl)methyl alcohol With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran; hexane Wittig type reaction; 8 h; Inert atmosphereReflux; optical yield given as percent de;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
European Journal of Organic Chemistry, 2009 , # 34 p. 6034 - 6042
1: (4-Methylphenyl)-magnesium bromide With [Ni0(1,5-cyclooctadiene)2]; SIDip*HCl in tetrahydrofuran T=0°C; 0.166667 h; 2: 1-(2-phenylsulfanylethyl)benzene in tetrahydrofuran T=0 - 60°C; 6.16667 h;
参考文献
Ishizuka, Kentaro; Seike, Hirofumi; Hatakeyama, Takuji; Nakamura, Masaharu
Journal of the American Chemical Society, 2010 , vol. 132, # 38 p. 13117 - 13119
