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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
472-65-1
合成路线
（共 10 条）
472-66-2
2,6,6-三甲基-1-环己烯基乙醛
→
反应条件
472-65-1
反应条件
sodium tetrahydroborate in methanol T=0 - 20°C; 1 h;
参考文献
Wang, Chuan; Yamamoto, Hisashi
Journal of the American Chemical Society, 2014 , vol. 136, # 4 p. 1222 - 1225
472-66-2
2,6,6-三甲基-1-环己烯基乙醛
→
反应条件
15356-74-8
二氢猕猴桃内酯
+
472-65-1
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
58937-20-5
→
反应条件
15356-74-8
二氢猕猴桃内酯
+
472-65-1
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
79-77-6
β-紫罗酮
→
反应条件
17283-81-7
BETA-二氢紫罗兰酮
+
60814-40-6
+
472-65-1
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in water T=28°C; 96 h; biotransformation at pH=6.2-6.5; Mechanism;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
79-77-6
β-紫罗酮
→
反应条件
27185-79-1
+
14398-34-6
+
60814-40-6
+
472-65-1
+
83646-52-0
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in water T=28°C; 6 h; biotransformation at pH=6.2-6.5; Mechanism;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
472-65-1
→
反应条件
83646-52-0
+
75203-87-1
反应条件
pyridine 1-oxide; selenium(IV) oxide in 1,4-dioxane T=85°C; 6 h;
参考文献
Aranda, Gerard; Bertranne-Delahaye, Mireille; Azerad, Robert; Maurs, Michele; Cortes, Manuel; Ramirez, Hector; Vernal, Gonzalo; Prange, Thierry
Synthetic Communications, 1997 , vol. 27, # 1 p. 45 - 60
472-65-1
→
反应条件
60814-40-6
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; 72 h; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
472-65-1
→
反应条件
83646-52-0
+
75203-87-1
反应条件
pyridine 1-oxide; selenium(IV) oxide in 1,4-dioxane T=85°C; 6 h;
参考文献
Aranda, Gerard; Bertranne-Delahaye, Mireille; Azerad, Robert; Maurs, Michele; Cortes, Manuel; Ramirez, Hector; Vernal, Gonzalo; Prange, Thierry
Synthetic Communications, 1997 , vol. 27, # 1 p. 45 - 60
472-65-1
→
反应条件
60814-40-6
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; 72 h; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
472-65-1
→
反应条件
反应条件
enzymatic hydroxylation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
