联苯-4,4-草酸二乙酯合成路线 （共 84 条）
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
N-ethyl-N,N-diisopropylamine; lithium chloride; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide T=100°C; 1.5 h; Product distribution; Further Variations:Reagentsreaction time;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Gavazza, Federica; Goggiamani, Antonella
Organic Letters, 2003 , vol. 5, # 3 p. 289 - 291
反应条件
1: 3-buten-2-yl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 4-iodobenzoic acid ethyl ester in N,N-dimethyl-formamide T=100°C; Title compound not separated from byproducts;
参考文献
Lee, Phil Ho; Seomoon, Dong; Lee, Kooyeon; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Sridhar, Madabhushi
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1641 - 1645
反应条件
[2,2']bipyridinyl; 1-acetoxy-2-methyl-buta-1,3-diene; trifluoroacetic acid; manganese; cobalt(II) dibromide in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne; Perichon, Jacques
European Journal of Organic Chemistry, 2005 , # 6 p. 989 - 992
反应条件
1: With 4-bromo-benzoic acid ethyl ester; trifluoroacetic acid; cobalt(II) dibromide; zinc in 1.4-dicyano 1-butene; acetonitrile 0.166667 - 0.5 h; 2: 4-bromo-benzoic acid ethyl ester With zinc dibromide in 1.4-dicyano 1-butene; acetonitrile Product distribution / selectivity;
参考文献
Perichon, Jacques; Gosmini, Corinne; Fillon, Hyacinthe
Patent: US2004/236155 A1, 2004 ;
Location in patent: Page 6; 7 ;
反应条件
1: 4-ethoxycarbonylphenylzinc iodide With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 5 h; 2: 1,4-Diiodobenzene With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 10 h; 3: With iodine in various solvent(s)
参考文献
Hossain, Kabir M.; Kameyama, Toru; Shibata, Takanori; Takagi, Kentaro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2415 - 2420
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; zinc; Co(2,2'-bipyridine)Br2 in pyridine; N-dodecane; acetonitrile T=50°C; 2.5 h; Title compound not separated from byproducts;
参考文献
Kazmierski, Igor; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Synlett, 2006 , # 6 p. 881 - 884
