联苯-4,4-草酸二乙酯合成路线 （共 84 条）
反应条件
1: 74 percent Chromat. / Zn; allyl chloride; TFA / CoBr2(2,2'-bipyridine) / acetonitrile; pyridine; dodecane / 21 h / 50 °C 2: pyridine / 0 - 20 °C 3: 19 percent Chromat. / Zn; allyl chloride; TFA / CoBr2(2,2'-bipyridine) / acetonitrile; pyridine; dodecane / 2.5 h / 50 °C View Scheme
参考文献
Kazmierski, Igor; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Synlett, 2006 , # 6 p. 881 - 884
反应条件
1: pyridine / 0 - 20 °C 2: 19 percent Chromat. / Zn; allyl chloride; TFA / CoBr2(2,2'-bipyridine) / acetonitrile; pyridine; dodecane / 2.5 h / 50 °C View Scheme
参考文献
Jutand, Anny; Mosleh, Adil
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 261 - 274
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 T=80°C; Substitution; 24 h;
参考文献
Hossain, Kabir M.; Takagi, Kentaro
Chemistry Letters, 1999 , # 11 p. 1241 - 1242
反应条件
bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; triphenylphosphine in toluene T=90°C; 12 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
反应条件
indium(III) chloride; indium; dimethyl(n-butyl)amine; tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
反应条件
triethylamine; palladium diacetate T=100°C; Heck reaction; 24 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; De Salve, Ilse; Fabrizi, Giancarlo
Synlett, 2006 , # 18 p. 2947 - 2952
反应条件
triethylamine; palladium diacetate T=100°C; Heck reaction; 24 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; De Salve, Ilse; Fabrizi, Giancarlo
Synlett, 2006 , # 18 p. 2947 - 2952
反应条件
thionyl chloride T=20°C; Reflux;
参考文献
Conejo-Garcia, Ana; Pisani, Leonardo; Del Carmen Nunez, Maria; Catto, Marco; Nicolotti, Orazio; Leonetti, Francesco; Campos, Joaquin M.; Gallo, Miguel A.; Espinosa, Antonio; Carotti, Angelo
Journal of Medicinal Chemistry, 2011 , vol. 54, # 8 p. 2627 - 2645
反应条件
chromium dichloride; manganese; chloro-trimethyl-silane; tetrabutyl ammonium fluoride; benzaldehyde; nickel dichloride 1.) DMF, DME, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Fuerstner, Alois; Shi, Nongyuan
Journal of the American Chemical Society, 1996 , vol. 118, # 10 p. 2533 - 2534
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate; cobalt(II) dibromide in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
