4,4’-(1,6-己二氧基)二苯胺合成路线 （共 12 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=80°C; P=5171.48 Torr; 3 h;
参考文献
Choi, E-Joon; Ahn, Jae-Chul; Chien, Liang-Chy; Lee, Chong-Kwang; Zin, Wang-Cheol; Kim, Dae-Cheol; Shin, Sung-Tae
Macromolecules, 2004 , vol. 37, # 1 p. 71 - 78
反应条件
sodium hydroxide in ethanol
参考文献
Henderson, Peter A.; Imrie, Corrie T.
Macromolecules, 2005 , vol. 38, # 8 p. 3307 - 3311
反应条件
1: 83 percent / K2CO3 / acetone
2: 92 percent / NaOH / ethanol
View Scheme
参考文献
Henderson, Peter A.; Imrie, Corrie T.
Macromolecules, 2005 , vol. 38, # 8 p. 3307 - 3311
反应条件
1: 72 percent / dimethylformamide / 10 h / Heating
2: H2 / 5percent Pd/C / tetrahydrofuran; methanol / 2280 Torr
View Scheme
参考文献
Turner, William R.; Werbel, Leslie M.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1728 - 1740
反应条件
1: 83 percent / K2CO3 / acetone
2: 92 percent / NaOH / ethanol
View Scheme
参考文献
Henderson, Peter A.; Imrie, Corrie T.
Macromolecules, 2005 , vol. 38, # 8 p. 3307 - 3311
反应条件
sodium hydrogencarbonate in water
1 h;
参考文献
Griffin; Britt; Hung; Steele
Molecular crystals and liquid crystals, 1983 , vol. 105, # 1-4 p. 305 - 314
反应条件
1: potassium carbonate / acetone / Heating
2: water; sodium hydroxide / ethanol / Heating
View Scheme
参考文献
Donaldson, Toby; Henderson, Peter A.; Achard, Marie France; Imrie, Corrie T.
Journal of Materials Chemistry, 2011 , vol. 21, # 29 p. 10935 - 10941
反应条件
platinum
Hydrogenation;
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
反应条件
1: potassium carbonate; butanone; potassium iodide
2: platinum / Hydrogenation
View Scheme
参考文献
Bergel; Reiner
Journal of the Chemical Society, 1959 , p. 2890,2891, 2892
反应条件
1: acetone
2: SnCl2; aqueous HCl; acetic acid
3: platinum / Hydrogenation
View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
