1,4,7-三氮杂环壬烷合成路线 （共 26 条）
反应条件
4-(N,N-dimethlyamino)pyridine in 1,4-dioxane 12 h; Heating;
参考文献
Walf, G. Henning; Benda, Ruediger; Litterst, F. Jochen; Stebani, Uwe; Schmidt, Steven; Lattermann, Guenter
Chemistry - A European Journal, 1998 , vol. 4, # 1 p. 93 - 99
参考文献
Lattermann, G.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 182, p. 299 - 311
反应条件
sodium hydroxide; hexadecylamine hydrochloride in water T=20°C; Condensation; 24 h;
参考文献
Tamura, Masakazu; Urano, Yasuteru; Kikuchi, Kazuya; Higuchi, Tsunehiko; Hirobe, Masaaki; Nagano, Tetsuo
Journal of Organometallic Chemistry, 2000 , vol. 611, # 1-2 p. 586 - 592
参考文献
Tsukube, Hiroshi; Yamashita, Kouichi; Iwachido, Tadashi; Zenki, Michio
Tetrahedron Letters, 1989 , vol. 30, # 30 p. 3983 - 3986
反应条件
triethylamine; sodium iodide in ethanol Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1661 - 1665
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 8 p. 1662 - 1670
反应条件
potassium hydroxide
1) toluene, 80-90 deg C, 2-3 h, 2) 80-90 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Haselhorst, Gabriele; Stoetzel, Stefan; Strassburger, Anja; Walz, Wolfgang; Wieghardt, Karl; Nuber, Bernhard
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1993 , # 1 p. 83 - 90
反应条件
triethylamine; trichlorophosphate in benzene
2 h; Ambient temperature;
参考文献
Bourne, Susan A.; Mbianda, Xavier Y.; Modro, Tomasz A.; Nassimbeni, Luigi R.; Wan, Huijie
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 1 p. 83 - 88
反应条件
(i) tris(dimethylamino)phosphine, toluene, (ii) sulfur; Multistep reaction;
参考文献
White,D.W. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 4921 - 4925
反应条件
(i) tris(dimethylamino)phosphine, toluene, (ii) Se; Multistep reaction;
参考文献
White,D.W. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 4921 - 4925
