1-甲基-2-(2-甲基苯氧基)苯合成路线 （共 16 条）
反应条件
sulfuric acid
T=95°C; Diazotization;
参考文献
Chatterjee
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 410,413
反应条件
potassium hydroxide; tri-n-butyl-antimony
1.) CH3CN, rt, 1 d, 2.) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Akiba, Kin-ya; Shimizu, Akiyoshi; Ohnari, Hideyuki; Ohkata, Katsuo
Tetrahedron Letters, 1985 , vol. 26, # 27 p. 3211 - 3214
反应条件
bei der trocknen Destillation;
参考文献
Moehlau
Chemische Berichte, 1916 , vol. 49, p. 169
Full Text Show Details
Gladstone; Tribe
Journal of the Chemical Society, 1886 , vol. 49, p. 29
Full Text Show Details
Russig
Z. Ang., 1919 , vol. 32, p. 39
反应条件
1: 95 percent / bromine / acetic acid / 0 °C
2: 79 percent / pyridine / 42 h / 230 °C / 1.) dry pyridine, 230 deg C, 42 h, 2.) ice, liquor ammonia, 3 h
View Scheme
参考文献
Chauhan, P. M.; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 898 - 900
反应条件
1: 95 percent / bromine / acetic acid / 0 °C
2: 79 percent / pyridine / 42 h / 230 °C / 1.) dry pyridine, 230 deg C, 42 h, 2.) ice, liquor ammonia, 3 h
3: 77 percent / NBS, dibenzoyl peroxide / CCl4 / 36 h / Heating; Irradiation
View Scheme
参考文献
Chauhan, P. M.; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 898 - 900
反应条件
1: 95 percent / bromine / acetic acid / 0 °C
2: 79 percent / pyridine / 42 h / 230 °C / 1.) dry pyridine, 230 deg C, 42 h, 2.) ice, liquor ammonia, 3 h
3: 75 percent / hydroxylamine hydrochloride, Na2CO3 / pyridine; ethanol; H2O / 3 h / Heating
View Scheme
参考文献
Chauhan, P. M.; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 898 - 900
