反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; phosphorus trichoride 1.) hexane, from 45 deg C to 50 deg C, 30 min, 2.) THF, -70 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Muller, Alfred; Otto, Stefanus; Roodt, Andreas
Dalton Transactions, 2008 , # 5 p. 650 - 657