2-氧代-N,2-二苯基-乙酰胺合成路线 （共 41 条）
反应条件
water in chloroform
T=20°C;
参考文献
Novikov, Mikhail S.; Voznyi, Igor V.; Khlebnikov, Alexander F.; Kopf, Juergen; Kostikov, Rafael R.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 14 p. 1628 - 1630
反应条件
potassium hydroxide in methanol; water
Heating;
参考文献
Haddadin, Makhluf J.; Kattan, Asma M.; Freeman, Jeremiah P.
Journal of Organic Chemistry, 1982 , vol. 47, # 4 p. 723 - 725
反应条件
1: sodium hydroxide; thionyl chloride / N,N-dimethyl acetamide; water / 0.42 h / -5 °C / |Inert atmosphere
2: N,N-dimethyl acetamide; water / 1 h / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Cvetovich, Raymond J.; DiMichele, Lisa
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 944 - 946
反应条件
in methanol
2 h; Heating;
参考文献
Boryczka, Stanislaw; Suwinska, Kinga; Le Guillanton, Georges; Do, Quang Tho; Elothmani, Driss
Journal of Chemical Crystallography, 1998 , vol. 28, # 7 p. 555 - 560
反应条件
1: 73 percent / sodium methoxide / methanol / overnight
2: 91 percent / 10N HCl / ethanol / 1 h / Heating
3: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
4: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
反应条件
1: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
2: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
反应条件
1: 91 percent / 10N HCl / ethanol / 1 h / Heating
2: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
3: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
反应条件
1: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
2: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
反应条件
1: 56 percent / aq. ethanol / 8 h / Heating
2: 73 percent / sodium methoxide / methanol / overnight
3: 91 percent / 10N HCl / ethanol / 1 h / Heating
4: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
5: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
反应条件
1: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating
2: 58 percent / 0.08 h / steam bath
View Scheme
参考文献
Ibrahim, Y. A.; Eid, M. M.; Badawy, M. A.; Abdel-Hady, S. A. L.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 953 - 956
