(3,4-二甲氧基苯基)-乙醛酸合成路线 （共 24 条）
反应条件
1: 93 percent / toluene / Heating
2: 47 percent / acetic acid / 5 h
3: 51 percent / 20percent aq. sodium hydroxide / dioxane / 48 h
View Scheme
参考文献
Lenz, George R.; Costanza, Carl; Lessor, Ralph A.; Ezell, Edward F.
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1753 - 1757
反应条件
1: 47 percent / acetic acid / 5 h
2: 51 percent / 20percent aq. sodium hydroxide / dioxane / 48 h
View Scheme
参考文献
Lenz, George R.; Costanza, Carl; Lessor, Ralph A.; Ezell, Edward F.
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1753 - 1757
反应条件
hydrogenchloride
T=20°C;
参考文献
Mauthner
Chemische Berichte, 1909 , vol. 42, p. 194
反应条件
potassium permanganate
T=80 - 90°C;
参考文献
Tiemann; Matsmoto
Chemische Berichte, 1878 , vol. 11, p. 143
参考文献
Glennie et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 2409,2410
反应条件
potassium permanganate; water; potassium carbonate
参考文献
Ciamician; Silber
Chemische Berichte, 1890 , vol. 23, p. 1165
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Kolokolow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1897 , vol. 29, p. 23
Chem. Zentralbl., 1897 , vol. 68, # I p. 915
反应条件
1: diethyl ether; pyridine
2: fuming hydrochloric acid / 20 °C
View Scheme
参考文献
Mauthner
Chemische Berichte, 1909 , vol. 42, p. 194
反应条件
1: chromic acid
2: KMnO4; alkali
View Scheme
参考文献
Bougault
Annales de Chimie (Cachan, France), 1902 , vol. <7> 25, p. 548
反应条件
potassium permanganate
constitution;
参考文献
Rao, Koppaka V.; Alvarez, Francisco M.
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4947 - 4950
参考文献
Mauthner
Chemische Berichte, 1909 , vol. 42, p. 194
