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1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2: 10 palladium on activated charcoal; hydrogen / ethanol 3: hydrogenchloride; sodium nitrite / water / Cooling with ice View Scheme

aluminum oxide; potassium fluoride; palladium T=100°C; Suzuki coupling; 4 h;

1.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2.1: 10 palladium on activated charcoal; hydrogen / ethanol 3.1: hydrogenchloride; sodium nitrite / water / Cooling with ice 4.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C 5.1: potassium hydrogen fluoride / methanol; water / 0.5 h 5.2: 1 h View Scheme

benzene unter Entfernen des entstehenden H2O;

dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate in toluene Suzuki coupling;