反应条件
1: hydrogen / palladium 10 on activated carbon / ethanol / 5 h / 2585.81 Torr
2: chloro-trimethyl-silane; trimethylphenylammonium monobromide; lithium hexamethyldisilazane / tetrahydrofuran / 1.33 h / -78 - 0 °C
3: dichloromethane / 0.5 h / 0 °C
4: N-ethyl-N,N-diisopropylamine / acetonitrile
View Scheme
参考文献
Walker, Daniel Patrick; Piotrowski, David W.; Jacobsen, Eric Jon; Acker, Brad A.; Myers, Jason K.; Groppi JR., Vincent E.
Patent: US2003/236279 A1, 2003 ;
