(2S,4r)-4-boc-氨基吡咯烷-2-羧酸甲酯合成路线 (共 11 条)
反应条件
methanol; palladium on activated charcoal
参考文献
Umashankara; Babu, I Ramesh; Ganesh, Krishna N
Chemical communications (Cambridge, England), 2003 , # 20 p. 2606 - 2607
反应条件
1: 60 percent / PPh3; DIAD / tetrahydrofuran 2: 90 percent / NaN3 / dimethylformamide 3: 93 percent / H2; Ni / ethyl acetate 4: 98 percent / methanol; Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686
反应条件
1: 93 percent / H2; Ni / ethyl acetate 2: 98 percent / methanol; Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686
反应条件
1: pyridine 2: 97 percent / LiN3 3: H2S / pyridine 4: DIEA 5: H2 / Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686
反应条件
1: 97 percent / LiN3 2: H2S / pyridine 3: DIEA 4: H2 / Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686
反应条件
1: NaOMe / methanol 2: pyridine 3: 97 percent / LiN3 4: H2S / pyridine 5: DIEA 6: H2 / Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686
反应条件
1: 98 percent / NaHCO3 / H2O 2: 94 percent / SOCl2 3: 60 percent / PPh3; DIAD / tetrahydrofuran 4: 90 percent / NaN3 / dimethylformamide 5: 93 percent / H2; Ni / ethyl acetate 6: 98 percent / methanol; Pd/C View Scheme
参考文献
Umashankara; Babu, I Ramesh; Ganesh, Krishna N
Chemical communications (Cambridge, England), 2003 , # 20 p. 2606 - 2607
反应条件
1: 94 percent / SOCl2 2: 60 percent / PPh3; DIAD / tetrahydrofuran 3: 90 percent / NaN3 / dimethylformamide 4: 93 percent / H2; Ni / ethyl acetate 5: 98 percent / methanol; Pd/C View Scheme
参考文献
Umashankara; Babu, I Ramesh; Ganesh, Krishna N
Chemical communications (Cambridge, England), 2003 , # 20 p. 2606 - 2607
反应条件
1: 90 percent / NaN3 / dimethylformamide 2: 93 percent / H2; Ni / ethyl acetate 3: 98 percent / methanol; Pd/C View Scheme
参考文献
Umashankara; Babu, I Ramesh; Ganesh, Krishna N
Chemical communications (Cambridge, England), 2003 , # 20 p. 2606 - 2607
反应条件
1: DIEA 2: H2 / Pd/C View Scheme
参考文献
Jordan, Stephan; Schwemler, Christoph; Kosch, Winfried; Kretschmer, Axel; Schwenner, Eckhardt; Stropp, Udo; Mielke, Burkhard
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 6 p. 681 - 686